Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Chloroquinoline → 4-Chloro-3,8-dimethyl-1-(2-quinolinyl)-1H-pyrazolo[3,4-b]quinoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Chloroquinoline | HCID 11928 | — |
| 반응물 | 2(1H)-Quinolinone, hydrazone | HCID 85111 | — |
| 반응물 | 8-methyl-2-(2-oxopropyl)-4H-3,1-benzoxazin-4-one | HCID 22320304 | — |
| 생성물 | 4-Chloro-3,8-dimethyl-1-(2-quinolinyl)-1H-pyrazolo[3,4-b]quinoline | HCID 22320348 | — |
반응 단계
Following the procedures described in Reference Example 1-10 and Example 1-34, the title compound was prepared from 8-methyl-2-(2-oxopropyl)-4H-3,1-benzoxazin-4-one and 2-hydrazinoquinoline which was separately prepared from 2-chloroquinoline following the method described in Reference Example 1-9 (42% yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06949648B2 |
| 출처 데이터셋 | uspto-grants-2005_09 |
| ORD ID | ord-ad094011bd7e4db1b874ef890b077745 |
| 출처 메모 | uspto-grants-2005_09 |