Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Nitro-n-[1-(4-pyridyl)piperidin-4-ylmethyl]pyridine-2-amine → N2-[1-(4-pyridyl)piperidin-4-ylmethyl]-2,3-pyridinediamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Nitro-n-[1-(4-pyridyl)piperidin-4-ylmethyl]pyridine-2-amine | HCID 23497755 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | N2-[1-(4-pyridyl)piperidin-4-ylmethyl]-2,3-pyridinediamine | HCID 12150690 | 97.1% |
반응 단계
Using a similar procedure to that described in Example 2, Part C, 3-nitro-N-[1-(4-pyridyl)piperidin-4-ylmethyl]pyridine-2-amine (340 mg, 1.09 mmol) and 10% palladium on carbon (200 mg) yielded 300 mg of the title compound, which was used without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06710057B2 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-03bbc50c157749ee9b5b92ccfd8c784d |
| 출처 메모 | uspto-grants-2004_03 |