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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 49947생성일: 2026년 10월 24일

Methyl iodide → Methyl 5-iodo-2-methoxybenzoate

https://huagongshe.com/ko/reaction/49947

반응식

참여 물질

역할이름HCID투입량
반응물Methyl iodideHCID 6328—
반응물Potassium CarbonateHCID 11430—
반응물Methyl 5-IodosalicylateHCID 248910—
용매DimethylformamideHCID 6228—
생성물Methyl 5-iodo-2-methoxybenzoateHCID 11011762—

반응 단계

Methyl iodide (0.29 ml, 4.68 mmol) was added to a mixture of 1.0 g (3.60 mmol) of methyl 5-iodosalicylate, 0.50 g (3.60 mmol) of potassium carbonate and 4 ml of dimethylformamide, and they were stirred at room temperature for 3 hours. The reaction mixture was filtered through Celite and then after-treated in by an ordinary method to obtain the title compound.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06710056B2
출처 데이터셋uspto-grants-2004_03
ORD IDord-fa15a67265c94805a97b2ae90bc289f0
출처 메모uspto-grants-2004_03