Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → Methyl 5-iodo-2-methoxybenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Methyl 5-Iodosalicylate | HCID 248910 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Methyl 5-iodo-2-methoxybenzoate | HCID 11011762 | — |
반응 단계
Methyl iodide (0.29 ml, 4.68 mmol) was added to a mixture of 1.0 g (3.60 mmol) of methyl 5-iodosalicylate, 0.50 g (3.60 mmol) of potassium carbonate and 4 ml of dimethylformamide, and they were stirred at room temperature for 3 hours. The reaction mixture was filtered through Celite and then after-treated in by an ordinary method to obtain the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06710056B2 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-fa15a67265c94805a97b2ae90bc289f0 |
| 출처 메모 | uspto-grants-2004_03 |