Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium → 5-Methyl-6-oxoheptanesulfonic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium | HCID 5360545 | — |
| 반응물 | 5-(Ethoxycarbonyl)-5-methyl-6-oxoheptane-1-sulphonate | HCID 59422465 | — |
| 용매 | Hydrochloric Acid | HCID 313 | — |
| 생성물 | 5-Methyl-6-oxoheptanesulfonic acid | HCID 57903351 | — |
반응 단계
5-(Ethoxycarbonyl)-5-methyl-6-oxoheptane-1-sulphonate, sodium salt (from 1.1) was heated at 90° C. in concentrated hydrochloric acid (200 ml), until TLC indicated complete reaction (˜3 hrs). The solvent was then evaporated under vacuum; the residue was purified by flash chromatography (Silica. Ethanol/dichloromethane mixtures) to give 49.6 g of 5-methyl-6-oxoheptane-1-sulphonic acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07767829B2 |
| 출처 데이터셋 | uspto-grants-2010_08 |
| ORD ID | ord-d343bf7b98de416fb47c01395140dd59 |
| 출처 메모 | uspto-grants-2010_08 |