Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrazine, [4-[(trifluoromethyl)thio]phenyl]- → HCID 58731518, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrazine, [4-[(trifluoromethyl)thio]phenyl]- | HCID 10420564 | — |
| 반응물 | 5-Methyl-6-oxoheptanesulfonic acid | HCID 57903351 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | HCID 58731518 | HCID 58731518 | 14.2% |
반응 단계
To 4-(trifluoromethylthio)phenylhydrazine (1 g) in acetic acid (40 ml) was added 5-methyl-6-oxoheptane-1-sulphonic acid (1.4 g) and the solution heated to reflux overnight. The volatiles were removed on a rotary evaporator to give the crude product, 1.1 g of which was purified by preparative HPLC. The relevant fractions were combined, concentrated on a rotary evaporator and freeze dried to give the desired product (260 mg). M+=381
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07767829B2 |
| 출처 데이터셋 | uspto-grants-2010_08 |
| ORD ID | ord-7773518b75a34179bcb983a4bc6863e6 |
| 출처 메모 | uspto-grants-2010_08 |