Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Bromostyrene → 4,4'-Dibromostilbene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Bromostyrene | HCID 16263 | — |
| 촉매 | HCID 178479819 | HCID 178479819 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 4,4'-Dibromostilbene | HCID 53395981 | — |
반응 단계
To a three neck 50 ml round bottom, 4-bromostyrene (14.490 g, 0.0786 mol) was added. To the solution, a magnetic stir bar along with dichloromethane (DCM) (10 mL) were added. To the solution, Grubb's catalyst (0.500 mg, 5.8×10−4 mol) along with DCM (25 mL) was added. The solution was allowed to react for 24 hours at room temperature. The precipitate was filtered and placed into a vial for storage.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07777176B2 |
| 출처 데이터셋 | uspto-grants-2010_08 |
| ORD ID | ord-7f80ae51b39a49fdba2b869075d15d29 |
| 출처 메모 | uspto-grants-2010_08 |