Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetone → HCID 57419464, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetone | HCID 180 | — |
| 반응물 | Dimethyl Sulfate | HCID 6497 | — |
| 반응물 | 3,5-Diiodosalicylic acid | HCID 8631 | — |
| 생성물 | HCID 57419464 | HCID 57419464 | — |
반응 단계
A mixture of 2-hydroxy-3,5-diiodobenzoic acid (3.9 g, 10.0 mmol) potassium carbonate (4.15 g, 30.0 mmol) and dimethyl sulfate (2.77 g, 22.0 mmol) in acetone (33 ml) was heated at reflux for 16 h, cooled and concentrated. The residue was dissolved in EtOAc and washed with water, brine, dried (Na2SO4), filtered and concentrated to give an off-white solid (4.2 g, quantitative yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09095590B2 |
| 출처 데이터셋 | uspto-grants-2015_08 |
| ORD ID | ord-e6ee1f4f5e034f97afe232c2fb260e3c |
| 출처 메모 | uspto-grants-2015_08 |