Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cinnamoyl Chloride → (E)-5-Cyano-1-(2-pyridyl)-2-styryl-1H-benzimidazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cinnamoyl Chloride | HCID 5354261 | — |
| 반응물 | (E)-1-(2-pyridyl)-2-styryl-1H-benzimidazole | HCID 9796241 | — |
| 반응물 | 2-amino-4-cyano-N-(2-pyridyl)aniline | HCID 22736644 | — |
| 생성물 | (E)-5-Cyano-1-(2-pyridyl)-2-styryl-1H-benzimidazole | HCID 22736679 | — |
반응 단계
(E)-5-Cyano-1-(2-pyridyl)-2-styryl-1H-benzimidazole was prepared from 2-amino-4-Cyano-N-(2-pyridyl)aniline and (E)-cinnamoyl chloride according to the preparation of (E)-1-(2-pyridyl)-2-styryl-1H-benzimidazole (Example 1, method A). MW: 322.37; mp: 172.0-172.7° C.; 1H-NMR (CDCl3) δ: 8.80 (1H. ddd, J=4.8, 1.8, 0.7 Hz), 8.15-8.02 (2H, m), 8.05 (1H, d, J=16.0 Hz), 7.57-7.48 (6H, m), 7.42-7.33 (3H, m), 7.07 (1H, d, J=16.0 Hz).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06713482B2 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-6fddfcf6ae3d41d09565e188c024a50e |
| 출처 메모 | uspto-grants-2004_03 |