Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Hexanol → 2-Hexyl methanesulfonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Hexanol | HCID 12297 | — |
| 반응물 | Methanesulfonyl chloride | HCID 31297 | — |
| 생성물 | 2-Hexyl methanesulfonate | HCID 15369440 | — |
반응 단계
The title compound was prepared by following the general procedure of Example 43 for mesylation as a colorless oil (408 mg, 68%) from 2-hexanol (312 mg, 2.90 mmol) and methanesulfonyl chloride (500 mg, 4.40 mmol). 1H NMR (CDCl3, 300 MHz) δ0.89-0.94 (m, 3H), 1.31-1.43 (m, 5H), 1.57-1.71 (m, 4H), 2.99 (s, 3H), 4.76-4.82 (m, 1H) ppm.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06713471B1 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-59f6081212b546948c3be8343fc3cd12 |
| 출처 메모 | uspto-grants-2004_03 |