Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Methyl-1-pentanol → 3-Methyl-1-pentyl methanesulfonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Methyl-1-pentanol | HCID 11508 | — |
| 반응물 | Methanesulfonyl chloride | HCID 31297 | — |
| 생성물 | 3-Methyl-1-pentyl methanesulfonate | HCID 22735904 | — |
반응 단계
The title compound was prepared by following the general procedure of Example 43 for mesylation as a colorless oil (384 mg, 67%) from 3-methyl-1-pentanol (300 mg, 2.90 mmol) and methanesulfonyl chloride (500 mg, 4.40 mmol). 1H NMR (CDCl3, 300 MHz) δ0.86-0.95 (m, 6H), 1.15-1.25 (m, 1H), 1.33-1.42 (m, 1H), 1.51-1.60 (m, 2H), 1.76-1.84 (m, 1H), 3.00 (s, 3H), 4.23-4.31 (m, 2H) ppm.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06713471B1 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-e27cfb6552834923a9a940411aab37f9 |
| 출처 메모 | uspto-grants-2004_03 |