Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Methyl-1-pentanol → HCID 22736017, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Methyl-1-pentanol | HCID 12296 | — |
| 반응물 | Methanesulfonyl chloride | HCID 31297 | — |
| 생성물 | HCID 22736017 | HCID 22736017 | — |
반응 단계
The title compound was prepared by following the general procedure of Example 43 for mesylation as a colorless oil (620 mg, 63%) from 4-methyl-1-pentanol (511 mg, 5.00 mmol) and methanesulfonyl chloride (844 mg, 7.50 mmol). 1H NMR (CDCl3, 300 MHz) δ0.88 (d, 6H, J=4.7 Hz), 1.23-1.31 (m, 2H), 1.53-1.62 (m, 1H), 1.70-1.80 (m, 2H), 3.00 (s, 3H), 4.21 (t, 2H, J=6.6 Hz) ppm.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06713471B1 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-eb37cb96c3ac4a40b1d317c93abe9152 |
| 출처 메모 | uspto-grants-2004_03 |