Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tributylamine → 5-Butoxy-4-methyl-1,3-oxazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tributylamine | HCID 7622 | — |
| 반응물 | n-Butyl alpha-isocyanopropionate | HCID 11171108 | — |
| 용매 | Chlorobenzene | HCID 7964 | — |
| 생성물 | 5-Butoxy-4-methyl-1,3-oxazole | HCID 9877440 | — |
반응 단계
A continuously operated dividing wall column (4.8 m×64 mm) packed with 3×3 mm V2A Raschig rings and a dividing wall of height 2.4 m having 60 theoretical plates was charged with a mixture of 13.1% by weight of n-butyl α-isocyanopropionate (R1 =n-butyl, R2=methyl), 32.2% by weight of monochlorobenzene and 50.1% by weight of tri-n-butylamine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06713630B2 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-03fcb0d775cb4cc78bd97c5afc46059b |
| 출처 메모 | uspto-grants-2004_03 |