Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Methylacetophenone → (2E)-3-(Dimethylamino)-1-(3-methylphenyl)prop-2-en-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Methylacetophenone | HCID 11455 | — |
| 반응물 | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| 생성물 | (2E)-3-(Dimethylamino)-1-(3-methylphenyl)prop-2-en-1-one | HCID 19807213 | 35% |
반응 단계
The title compound was prepared in 35% yield from 1-(3-methylphenyl)ethanone and DMF-DMA according to the procedure for the preparation of Example 12, part A. 1H NMR (400 MHz, CDCl3): δ 2.39 (3H, s), 2.79-3.11 (6H, m), 5.70 (1H, d, J=12.4 Hz), 7.24-7.31 (2H, m), 7.66-7.71 (2H, m), 7.78 (1H, d, J=12.4 Hz).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09107916B2 |
| 출처 데이터셋 | uspto-grants-2015_08 |
| ORD ID | ord-2873005cdbc848fb862feddeea823865 |
| 출처 메모 | uspto-grants-2015_08 |