참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Chlorodimethylsilane | HCID 66108 | — |
| 반응물 | 4-Pentenoic acid, phenylmethyl ester | HCID 10052035 | — |
| 생성물 | Benzyl 5-(chlorodimethylsilyl)pentanoate | HCID 90417974 | — |
반응 단계
To a mixture of chlorodimethylsilane (0.730 g; 6.57 mmol) and benzyl pent-4-enoate (1.25 g; 6.57 mmol) under argon was added one drop of Karstedt's catalyst solution (in xylenes; ˜2% Pt). The reaction vessel was sealed and the mixture was heated to 60° C. for 13.5 hours. The crude liquid was used without purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US09352049B2 |
|---|
| 출처 데이터셋 | uspto-grants-2016_05 |
|---|
| ORD ID | ord-8f257ecde9994d4b96cd6c2c43e51915 |
|---|
| 출처 메모 | uspto-grants-2016_05 |
|---|
