Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → HCID 67316267, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 1-Naphthalenethiol | HCID 68259 | — |
| 반응물 | Ethyl 3-(3-(methylsulfonyloxy)propyl)-1h-indole-2-carboxylate | HCID 87353567 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | HCID 67316267 | HCID 67316267 | — |
반응 단계
A mixture of EXAMPLE 10A (42 mg), naphthalene thiol (45 mg), and potassium carbonate (36 mg) in acetonitrile (2 mL) was heated at 80° C. for 3 days. The reaction mixture was poured into water, extracted with dichloromethane and purified by flash chromatography on silica gel with 0-20% ethyl acetate in hexanes.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08853209B2 |
| 출처 데이터셋 | uspto-grants-2014_10 |
| ORD ID | ord-e1dfa09626a14fc0925b8340aa0a84fc |
| 출처 메모 | uspto-grants-2014_10 |