Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethylene Glycol → 2-(2-Bromophenyl)-1,3-dioxolane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethylene Glycol | HCID 174 | — |
| 반응물 | Toluene | HCID 1140 | — |
| 반응물 | 2-Bromobenzaldehyde | HCID 81129 | — |
| 반응물 | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| 생성물 | 2-(2-Bromophenyl)-1,3-dioxolane | HCID 553534 | — |
반응 단계
A 12 L 3-necked flask fitted with an overhead stirrer was charged with 2-bromobenzaldehyde (800 g, 4.324 moles), ethylene glycol (402.6 g, 6.485 moles), p-toluenesulfonic acid·H2O (3.95 g, 0.021 moles) and toluene (3.785 kg, 41.074 moles).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05618946 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-d9a0f3d8f7324362b0f38c8dd31215ac |
| 출처 메모 | uspto-grants-1997_04 |