Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Chloro-2-phenyl-pyrimidine-5-carboxylic acid benzylamide → HCID 178418303, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Chloro-2-phenyl-pyrimidine-5-carboxylic acid benzylamide | HCID 53937500 | — |
| 반응물 | Sodium hydrogen sulphide | HCID 86586439 | — |
| 생성물 | HCID 178418303 | HCID 178418303 | 65.2% |
반응 단계
Using the procedure from Preparation 34, 5.8 g (17.9 mmol) of 4-chloro-2-phenyl-pyrimidine-5-carboxylic acid benzylamide was reacted with 5.1 g (72 mmol) of sodium hydrogen sulfide to give 3.75 g of the title compound, mp 189°-193° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05620997 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-b581ef5d5aa04389b56c7219e4b33d96 |
| 출처 메모 | uspto-grants-1997_04 |