Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Iodine → 2-Benzyl-6-phenyl-isothiazolo[5,4-d]pyrimidin-3-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Iodine | HCID 807 | — |
| 반응물 | HCID 178418303 | HCID 178418303 | — |
| 생성물 | 2-Benzyl-6-phenyl-isothiazolo[5,4-d]pyrimidin-3-one | HCID 23287902 | 87.6% |
반응 단계
Using the procedure of Example 20, 2.0 g (6.22 mmol) of 4-mercapto-2-phenyl-pyrimidine-5-carboxylic acid benzylamide (from Preparation 42) was reacted with 1.74 g (6.8 mmol) of iodine to give 1.74 g of the title compound after crystallization from isopropanol, mp 166°-167° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05620997 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-b44c82636d854ec29f3c95413e79d974 |
| 출처 메모 | uspto-grants-1997_04 |