Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethyl Sulfoxide → 1-(4-Chlorophenyl)-cyclopentanecarbaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethyl Sulfoxide | HCID 679 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | 1-(p-Chlorophenyl)cyclopentanemethanol | HCID 2724017 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 1-(4-Chlorophenyl)-cyclopentanecarbaldehyde | HCID 21468000 | — |
반응 단계
This compound is prepared in a manner analogous to that of Step B of Example 4, using 7.0 grams (0.055 mole) of oxalyl chloride, 9.5 grams (0.120 mole) of dimethyl sulfoxide, 10.5 grams (0.050 mole) of [1-(4-chlorophenyl)-1-cyclopentyl]methanol, and 25.5 grams (0.250 mole) of triethylamine in 175 mL of methylene chloride, yielding 1-(4-chlorophenyl)-1-cyclopentanecarboxaldehyde.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05622954 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-77961596412b4d11bac1cca180d2c59a |
| 출처 메모 | uspto-grants-1997_04 |