Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5,10-Dihydro-11H-dibenzo(b,e)(1,4)diazepin-11-one → 5,10-dihydro-5-[(1,5-dimethyl-1,2,5,6-tetrahydro-4-pyridinyl)-carbonyl]-11H-dibenzo[b,e][1,4]diazepin-11-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5,10-Dihydro-11H-dibenzo(b,e)(1,4)diazepin-11-one | HCID 201327 | — |
| 반응물 | 5,10-dihydro-5[(3-methyl-4-pyridinyl)carbonyl]-11H-dibenzo[b,e][1,4]-diazepin-11-one | HCID 13285863 | — |
| 반응물 | 3-Methylpyridine-4-carbonyl chloride | HCID 13285864 | — |
| 반응물 | Benzo[b][1,4]benzodiazepin-6-one | HCID 19781529 | — |
| 반응물 | Diisopropylether methanol | HCID 21882575 | — |
| 생성물 | 5,10-dihydro-5-[(1,5-dimethyl-1,2,5,6-tetrahydro-4-pyridinyl)-carbonyl]-11H-dibenzo[b,e][1,4]diazepin-11-one | HCID 20460470 | — |
반응 단계
By reacting 5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one with 3-methylisonicotinic acid chloride (m.p. 155°-156° C.) via 5,10-dihydro-5-[3-methyl-4-pyridinyl)carbonyl]-11H-dibenzo[b,e][1,4]diazepin-11-one, m.p. 223°-224° C. (diisopropylether/methanol) and 5,10-dihydro-5[(3-methyl-4-pyridinyl)carbonyl]-11H-dibenzo[b,e][1,4]-diazepin-11-one methoiodide;
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04447434 |
| 출처 데이터셋 | uspto-grants-1984_05 |
| ORD ID | ord-ed1696b1d7f04771a91568d987f79a12 |
| 출처 메모 | uspto-grants-1984_05 |