Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Homoveratrylamine → N-[2-(3,4-dimethoxyphenyl)ethyl]-2-(N,N-diphenylamino)acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Homoveratrylamine | HCID 8421 | — |
| 반응물 | (Diphenylamino)acetic acid | HCID 735138 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | N-[2-(3,4-dimethoxyphenyl)ethyl]-2-(N,N-diphenylamino)acetamide | HCID 20460535 | 66.9% |
반응 단계
3,4-Dimethoxyphenethylamine (8.05 g) and N,N-diphenylglycine (10 g) were heated for 2 hours at 190° C. After cooling, the reaction mixture was dissolved in ethylacetate. The resulting solution was washed with a 5% sodium bicarbonate aqueous solution and water and then dried. The solvent was distilled off from the solution to give crystals of N-[2-(3,4-dimethoxyphenyl)ethyl]-2-(N,N-diphenylamino)acetamide (11.5 g), mp 88° to 93° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04447436 |
| 출처 데이터셋 | uspto-grants-1984_05 |
| ORD ID | ord-45297bd446e64c57a8b8e214217fb816 |
| 출처 메모 | uspto-grants-1984_05 |