돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 54587생성일: 2026년 10월 23일

Acetic Acid → 2-(4-tert-butylbenzylidene)-3,4-dihydro-1(2H)-naphthalenone

https://huagongshe.com/ko/reaction/54587

반응식

참여 물질

역할이름HCID투입량
반응물Acetic AcidHCID 176—
반응물1-TetraloneHCID 10724—
반응물Potassium HydroxideHCID 14797—
반응물4-tert-ButylbenzaldehydeHCID 70324—
용매MethanolHCID 887—
용매WaterHCID 962—
생성물2-(4-tert-butylbenzylidene)-3,4-dihydro-1(2H)-naphthalenoneHCID 3571213—

반응 단계

A mixture of 3,4-dihydro-1(2H)-naphthalenone (4.5 g) and 4-tert-butylbenzaldehyde (5.0 g) was stirred with a solution of 4% potassium hydroxide in methanol (100 ml) for 64 hours at room temperature. The mixture was neutralised with glacial acetic acid, followed by dilution with water (100 ml). The resulting copious white precipitate was filtered off, washed with water and dried in vacuo to give 2-(4-tert-butylbenzylidene)-3,4-dihydro-1(2H)-naphthalenone.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05622987
출처 데이터셋uspto-grants-1997_04
ORD IDord-392e6da757734f54a4b9ebfe00572a19
출처 메모uspto-grants-1997_04