Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Acid → 2-(4-tert-butylbenzylidene)-3,4-dihydro-1(2H)-naphthalenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | 1-Tetralone | HCID 10724 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | 4-tert-Butylbenzaldehyde | HCID 70324 | — |
| 용매 | Methanol | HCID 887 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2-(4-tert-butylbenzylidene)-3,4-dihydro-1(2H)-naphthalenone | HCID 3571213 | — |
반응 단계
A mixture of 3,4-dihydro-1(2H)-naphthalenone (4.5 g) and 4-tert-butylbenzaldehyde (5.0 g) was stirred with a solution of 4% potassium hydroxide in methanol (100 ml) for 64 hours at room temperature. The mixture was neutralised with glacial acetic acid, followed by dilution with water (100 ml). The resulting copious white precipitate was filtered off, washed with water and dried in vacuo to give 2-(4-tert-butylbenzylidene)-3,4-dihydro-1(2H)-naphthalenone.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05622987 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-392e6da757734f54a4b9ebfe00572a19 |
| 출처 메모 | uspto-grants-1997_04 |