Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Chloro-4-isocyanato-2-(trifluoromethyl) benzene → 1-[4-(2-Quinolylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)urea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Chloro-4-isocyanato-2-(trifluoromethyl) benzene | HCID 2733265 | — |
| 반응물 | 2-(4-Aminophenylthio)quinoline | HCID 22637130 | — |
| 생성물 | 1-[4-(2-Quinolylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)urea | HCID 18971663 | — |
반응 단계
2-(4-Aminophenylthio)quinoline (3.9 moles, 1.0 g) and 4-chloro-3-trifluoromethylphenylisocyanate (3.9 moles, 0.85 g) were reacted according to procedure A to yield the title compound, 0.8 g, 43%. Mass Spec (FD) 463. Calculated for C23H15ClF3N3OS: C, 58.29; H, 3.19; N, 8.87. Found: C, 58.56; H, 3.43; N, 9.02. M Pt 194°-195 ° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05624937 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-edef4794f6394e139c3094c299faa755 |
| 출처 메모 | uspto-grants-1997_04 |