Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Guanidine Hydrochloride → HCID 178478910, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Guanidine Hydrochloride | HCID 5742 | — |
| 반응물 | Methyl 1-methyl-1H-indole-5-carboxylate | HCID 10679201 | — |
| 반응물 | Sodium Methoxide | HCID 10942334 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | HCID 178478910 | HCID 178478910 | 68.9% |
반응 단계
The reaction was carried out in a manner similar to Example 1 except for using 1.00 g (5.29 mmol) of methyl 1-methyl-5-indolecarboxylate, 5.05 g (52.9 mmol) of guanidine hydrochloride and 50 ml of a methanol solution of 2.85 g (52.9 mmol) of sodium methoxide. Thus 0.92 g (68.9%) of 1-methyl-5-indoloylguanidine hydrochloride was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06169107A |
| 출처 데이터셋 | uspto-grants-2001_01 |
| ORD ID | ord-79b75a0701a94757837a47f7f0a1043e |
| 출처 메모 | uspto-grants-2001_01 |