Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzoic acid, 4-amino-, 1,1-dimethylethyl ester → Tert-butyl 4-(2-(4-(2,5-dichlorophenyl)-2-oxopyridin-1(2h)-yl)propanamido)benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzoic acid, 4-amino-, 1,1-dimethylethyl ester | HCID 233272 | — |
| 반응물 | 2-[4-(2,5-Dichlorophenyl)-2-oxopyridin-1(2H)-yl]propanoic acid | HCID 117622564 | — |
| 생성물 | Tert-butyl 4-(2-(4-(2,5-dichlorophenyl)-2-oxopyridin-1(2h)-yl)propanamido)benzoate | HCID 117622667 | — |
반응 단계
117 mg (0.36 mmol) of 2-[4-(2,5-dichlorophenyl)-2-oxopyridin-1(2H)-yl]propanoic acid (racemate) and 1.2 eq. of tert-butyl 4-aminobenzoate were reacted according to General Method 5A. Yield: 83 mg (47% of theory)
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09434690B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-7a827b9686aa4e8e877af8c33ecb9ff5 |
| 출처 메모 | uspto-grants-2016_09 |