Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pyridinium hydrochloride → 4-(5-Chloro-2-cyanophenyl)-6-oxo-1,6-dihydropyridin-3-carbonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pyridinium hydrochloride | HCID 21584435 | — |
| 반응물 | 4-(5-Chloro-2-cyanophenyl)-6-methoxypyridin-3-carbonitrile | HCID 117604910 | — |
| 생성물 | 4-(5-Chloro-2-cyanophenyl)-6-oxo-1,6-dihydropyridin-3-carbonitrile | HCID 117605665 | — |
반응 단계
414 mg (purity 94%, 1.14 mmol) of 4-(5-chloro-2-cyanophenyl)-6-methoxypyridin-3-carbonitrile and pyridinium hydrochloride were reacted according to General Method 3A. Yield: 312 mg (purity 91%, 77% of theory)
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09434690B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-286176a007e44eb3b6ad3ebd47ff8491 |
| 출처 메모 | uspto-grants-2016_09 |