참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Calcium Carbonate | HCID 10112 | — |
| 반응물 | 3-(1-Bromoethyl)benzophenone | HCID 12802924 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 3-(1-Hydroxyethyl)benzophenone | HCID 13102751 | — |
반응 단계
In an autoclave, 100 ml of water and 3.3 g of calcium carbonate and 10 g of 3-(1-bromoethyl)benzophenone were placed, and were then heated at 120° C. for 6 hours. The resultant reaction solution was extracted with benzene, and a formed benzene layer was then dried with anhydrous sodium sulfate, followed by distilling off the solvent. The resultant product had the spectrum data which were identical with those of 3-(1-hydroxyethyl)benzophenone.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04734528 |
|---|
| 출처 데이터셋 | uspto-grants-1988_03 |
|---|
| ORD ID | ord-fa741a064cc14d138e326f1101822562 |
|---|
| 출처 메모 | uspto-grants-1988_03 |
|---|
