Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → Methyl 4-amino-3-(4-chlorocinnamylamino)benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 3,5-Diamino-2-methylbenzoic acid | HCID 135524 | — |
| 반응물 | p-Chlorocinnamyl chloride | HCID 53728250 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Methyl 4-amino-3-(4-chlorocinnamylamino)benzoate | HCID 53813638 | 63.2% |
반응 단계
5.0 g of methyl 3,4-diaminobenzoate was dissolved in 40 ml of dimethylformamide, and to the solution were added 2.07 g of potassium carbonate and 1.87 g of p-chlorocinnamyl chloride, and reaction was carried out according to the procedure in Reference Example 40, to obtain 2.0 g of the title compound as a light brown oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05245034 |
| 출처 데이터셋 | uspto-grants-1993_09 |
| ORD ID | ord-02666c15032d4a23816abf9f01b6ac87 |
| 출처 메모 | uspto-grants-1993_09 |