Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Vinyl-2-trifluoromethyl-2,3,3-trifluorocyclobutane → Benzene, 1-fluoro-2-(trifluoromethyl)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Vinyl-2-trifluoromethyl-2,3,3-trifluorocyclobutane | HCID 20134582 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | Benzene, 1-fluoro-2-(trifluoromethyl)- | HCID 9807 | 41% |
반응 단계
The general procedure was followed using 11.0 g of 1-vinyl-2-trifluoromethyl-2,3,3-trifluorocyclobutane dissolved in 11.15 g of benzene as the liquid feed at a flow rate of 1 ml/hr. Nitrogen was used as the inert carrier. The reactor was charged with 2.0 g of activated carbon. At 400° C. 41% of o-trifluoromethylfluorobenzene was produced.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04754084 |
| 출처 데이터셋 | uspto-grants-1988_06 |
| ORD ID | ord-39825371865942a4b6ee94c2fdc6ef8a |
| 출처 메모 | uspto-grants-1988_06 |