Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dibenzo(b,d)thiophene-2-carbaldehyde → HCID 86695667, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dibenzo(b,d)thiophene-2-carbaldehyde | HCID 641360 | — |
| 반응물 | Ethyl 4-amino-4-(2,6-dimethoxyphenyl)-2-methylbutanoate | HCID 69085588 | — |
| 생성물 | HCID 86695667 | HCID 86695667 | — |
반응 단계
Prepared according to the described general procedure 2 (GP2) by reaction of ethyl 4-amino-4-(2,6-dimethoxyphenyl)-2-methylbutanoate with synthesized dibenzo[b,d]thiophene-2-carbaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=0.99 min.; [M+H]+: 431.87 g/mol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09242970B2 |
| 출처 데이터셋 | uspto-grants-2016_01 |
| ORD ID | ord-13b10fd70df04204a33dafa5c96e0e63 |
| 출처 메모 | uspto-grants-2016_01 |