Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Formaldehyde → Benzophenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Formaldehyde | HCID 712 | — |
| 반응물 | 8-chloro-1-[[(cyclopropylmethyl)methylamino]methyl]-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine | HCID 12612433 | — |
| 용매 | Formic Acid | HCID 284 | — |
| 생성물 | Benzophenone | HCID 3102 | — |
반응 단계
In the manner given in Example 1, 8-chloro-1-[[(cyclopropylmethyl)methylamino]methyl]-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine is heated in formic acid with aqueous formaldehyde to give 5-chloro-2-[3-[[(cyclopropylmethyl)methylamino]methyl]-5-](dimethylamino)methyl]-4-H-1,2,4-triazol-4-yl]benzophenone. This product is identical to that given in Example 21.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04010177 |
| 출처 데이터셋 | uspto-grants-1977_03 |
| ORD ID | ord-d54cecf16a37440894662ab6834afba9 |
| 출처 메모 | uspto-grants-1977_03 |