Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → p-Tetradecyloxyphenylacetylchloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | p-Tetradecyloxyphenylacetic acid | HCID 10472964 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | p-Tetradecyloxyphenylacetylchloride | HCID 10021844 | — |
반응 단계
A solution of 10.0 g. p-tetradecyloxyphenylacetic acid in 100 ml. absolute benzene is treated with 19.9 g thionylchloride and refluxed for 2.5 hours. The reaction mixture is then evaporated under vacuum (i.v.) and azeotroped several times with benzene to remove residual thionylchloride, to obtain crude p-tetradecyloxyphenylacetylchloride, which may be used in Step E, below, without further refining.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04011339 |
| 출처 데이터셋 | uspto-grants-1977_03 |
| ORD ID | ord-5e97ab17b6eb4490a02e2bd78e3b8f55 |
| 출처 메모 | uspto-grants-1977_03 |