Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → N-[(4s)-1-Azatricyclo[3.3.1.13,7]dec-4-yl]-4-phenoxybenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | 4-Phenoxybenzoic acid | HCID 75182 | — |
| 반응물 | 1-Azatricyclo[3.3.1.1,3,7]decan-4-amine | HCID 15686618 | — |
| 생성물 | N-[(4s)-1-Azatricyclo[3.3.1.13,7]dec-4-yl]-4-phenoxybenzamide | HCID 16068053 | — |
반응 단계
Prepared from (4s)-1-azatricyclo[3.3.1.13,7]dec-4-ylamine and 4-phenoxybenzoic acid (Aldrich) according to method B; 1H NMR (500 MHz, methanol-d4) δ 1.95 (d, J=13 Hz, 2H), 2.11 (s, 1H), 2.31 (d, J=13 Hz, 2H), 2.38 (s, 2H), 3.49 (s, 2H), 3.59 (s, 4H), 4.38 (s, 1H), 7.00-7.09 (m, 4H), 7.17-7.23 (m, 1H), 7.38-7.44 (m, J=8, 8 Hz, 2H), 7.81-7.89 (m, 2H); MS (APCI/NH3) m/z 349 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07897766B2 |
| 출처 데이터셋 | uspto-grants-2011_03 |
| ORD ID | ord-107ca2a23ef24a8dba551d095d9e7fe5 |
| 출처 메모 | uspto-grants-2011_03 |