Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Hydroxybenzonitrile → O-2-cyanophenyl dimethylthiocarbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Hydroxybenzonitrile | HCID 11907 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | Dimethylthiocarbamoyl chloride | HCID 27871 | — |
| 생성물 | O-2-cyanophenyl dimethylthiocarbamate | HCID 14795403 | 94% |
반응 단계
If the procedure described in Preparation XVI is followed starting from 15 g (126.10-3 mol) of 2-hydroxybenzonitrile, 17.9 g (145.10-3 mol) of dimethylthiocarbamoyl chloride and 7.4 g (126.10-3 mol) of potassium hydroxide, 24.1 g (yield: 94%) of the expected product are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05246961 |
| 출처 데이터셋 | uspto-grants-1993_09 |
| ORD ID | ord-0e3bf4991a3f466d9c41ae0105fc4554 |
| 출처 메모 | uspto-grants-1993_09 |