Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Mercuric cyanide → HCID 14795357, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Mercuric cyanide | HCID 11591 | — |
| 반응물 | 2-(Trifluoromethyl)benzenethiol | HCID 2777889 | — |
| 반응물 | 2,3,4-tri-O-acetyl-5-thio-alpha-xylopyranosyl bromide | HCID 10926314 | — |
| 생성물 | HCID 14795357 | HCID 14795357 | 34% |
반응 단계
If the procedure described in Preparation I is followed starting from 1.8 g (10.10-3 mol) of 2trifluoromethylbenzenethiol, 2.55 g (10.10-3 mol) of mercuric cyanide (Hg(CN)2) and 3.95 g (11.10-3 mol) of 2,3,4-tri-O-acetyl-5-thio-α-D-xylopyranosyl bromide, 1.53 g (yield: 34%) of the expected product are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05246961 |
| 출처 데이터셋 | uspto-grants-1993_09 |
| ORD ID | ord-b4d8de5548014418855293f67040f611 |
| 출처 메모 | uspto-grants-1993_09 |