Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl Ether → Butylnorbornene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | 2,6-Di-tert-butylpyridine | HCID 68510 | — |
| 반응물 | Lithium tetrakis(pentafluorophenyl)borate | HCID 23709652 | — |
| 촉매 | HCID 178455862 | HCID 178455862 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Butylnorbornene | HCID 19091267 | — |
반응 단계
A 50 weight percent solution of butylnorbornene (5.0 g, 0.033 mol) was prepared in toluene. Lithium tetrakis(pentafluorophenyl)borate.2.5 Et2O (0.0012 g, 0.0014 mmol) was combined with (allyl)palladiumchloride dimer (100 μl of a 1.4 mmol solution in toluene) and 2,6-di-t-butylpyridine (100 μl of a 2.9 mmol solution in toluene) in toluene and added to the monomer mixture. A polymeric puck formed within 5-10 min at room temperature.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07910674B2 |
| 출처 데이터셋 | uspto-grants-2011_03 |
| ORD ID | ord-8e01cb8cab4f4db095c7f89fde0a1d7c |
| 출처 메모 | uspto-grants-2011_03 |