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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 614021생성일: 2026년 10월 24일

Cyanide → 1-n-Butyl-3-(p-chloro-alpha,alpha-dimethylbenzyl)-1-ethylurea

https://huagongshe.com/ko/reaction/614021

반응식

참여 물질

역할이름HCID투입량
반응물CyanideHCID 5975—
반응물ButylethylamineHCID 25914—
반응물1-Chloro-4-(2-isocyanatopropan-2-yl)benzeneHCID 13118323—
용매Methyl Isobutyl KetoneHCID 7909—
생성물1-n-Butyl-3-(p-chloro-alpha,alpha-dimethylbenzyl)-1-ethylureaHCID 5444168386.2%

반응 단계

A solution of 3.9 g of p-chloro-α,α-dimethylbenzyl isocyanate, prepared from the corresponding cyanide in the same way as in Synthesis Example 1, in 20 ml of methyl isobutyl ketone was added to 2.2 g of N-n-butylethylamine. The solvent was then removed by distillation under reduced pressure and the resulting crystals were recrystallized from n-hexane to obtain 5.1 g of the title compound.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04143061
출처 데이터셋uspto-grants-1979_03
ORD IDord-c2dcf5310609440cb2e68c0e1dc319f3
출처 메모uspto-grants-1979_03