Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(cis-2,6-Dimethyl-1-piperidinyl)ethanamine → cis-N-[2-(2,6-dimethyl-1-piperidinyl)ethyl]-5,5-dimethyl-2-oxo-1-pyrrolidineacetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(cis-2,6-Dimethyl-1-piperidinyl)ethanamine | HCID 783702 | — |
| 반응물 | Ethyl 2,2-dimethyl-5-oxopyrrolidineacetate | HCID 21327791 | — |
| 생성물 | cis-N-[2-(2,6-dimethyl-1-piperidinyl)ethyl]-5,5-dimethyl-2-oxo-1-pyrrolidineacetamide | HCID 70609679 | — |
반응 단계
From 10 g. of ethyl 2,2-dimethyl-5-oxo-1-pyrrolidineacetate and 11 g. of cis-2-(2,6-dimethyl-1-piperidinyl)ethylamine, following the procedure of Example 9, there is obtained cis-N-[2-(2,6-dimethyl-1-piperidinyl)ethyl]-5,5-dimethyl-2-oxo-1-pyrrolidineacetamide as the hemihydrate; m.p. 94°-94.5° C. after recrystallization from isooctane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04145347 |
| 출처 데이터셋 | uspto-grants-1979_03 |
| ORD ID | ord-598508840ffa4da0adac05ffe4e0cd5b |
| 출처 메모 | uspto-grants-1979_03 |