Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetyl chloride → Methyl 3-(4-methylphenyl)-2-propenoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetyl chloride | HCID 6367 | — |
| 반응물 | 3-(p-Tolyl)acrylic acid | HCID 15835 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Methyl 3-(4-methylphenyl)-2-propenoate | HCID 589472 | — |
반응 단계
A solution of 6.0 g (37.0 mmol) of 4-methylcinnamic acid in 120 ml of anhydrous MeOH was treated with 6 ml of acetyl chloride and stirred at reflux for 18 hours. Evaporation of the MeOH gave the title ester as a white solid, mp 53.5°-57.5° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04499299 |
| 출처 데이터셋 | uspto-grants-1985_02 |
| ORD ID | ord-48020e780ce84bf2a68e8cb41673e567 |
| 출처 메모 | uspto-grants-1985_02 |