Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(3-Phthalimidopropyloxy)pyridine → 4-(3-Phthalimidopropyloxy)pyridine hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(3-Phthalimidopropyloxy)pyridine | HCID 19079090 | — |
| 반응물 | Hydrochloride methanol | HCID 21893726 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 4-(3-Phthalimidopropyloxy)pyridine hydrochloride | HCID 19079089 | 64.8% |
반응 단계
To a solution of 1.41 g (5.0 mmol) of 4-(3-phthalimidopropyloxy)pyridine in 20 ml of methanol, 10 ml of hydrogen chloride-methanol was added. The solvent was distilled off and acetone was added to the residue. The resulting crystals were collected by filtration and washed with acetone to give 1.03 g of the desired compound (64.8% yield, colorless crystals), mp. 167°-169° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05246948 |
| 출처 데이터셋 | uspto-grants-1993_09 |
| ORD ID | ord-c962e1c87c844b4594420eb59c04a717 |
| 출처 메모 | uspto-grants-1993_09 |