Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HCID 20368146, 화합물 → 1H-1,4-Benzodiazepine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | HCID 20368146 | HCID 20368146 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 용매 | Acetyl chloride | HCID 6367 | — |
| 생성물 | 1H-1,4-Benzodiazepine | HCID 148431 | — |
반응 단계
In the manner given in Example 1, a solution of 8-fluoro-1-methyl-6-(o-fluorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine in dimethylformamide, N,N,N',N'-tetrapropyldiaminomethane and acetyl chloride (in 0.5 molar excess compared to the N,N,N',N'-tetrapropyldiaminomethane) are reacted together to give 8-fluoro-1[2-(dipropylamino)ethyl]-6-(o-fluorophenyl)-4H-s-triazolo[4,3-a][1,4-benzodiazepine
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04075221 |
| 출처 데이터셋 | uspto-grants-1978_02 |
| ORD ID | ord-e375e263f104480eb2604e29d92efb05 |
| 출처 메모 | uspto-grants-1978_02 |