Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylformamide → 7-Methoxyheptanoic Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | 7-Bromoheptanoic acid | HCID 121723 | — |
| 생성물 | 7-Methoxyheptanoic Acid | HCID 15409528 | — |
반응 단계
The title compound was prepared by the method of Example 1 using 7-bromoheptanoic acid (50 g, 239 mmol) instead of 12-bromoundecanoic acid and dimethylformamide (300 mL) instead of methanol as the solvent. Concentration afforded the title compound (30 g) as a pale yellow liquid and the structure verified by NMR.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05952377 |
| 출처 데이터셋 | uspto-grants-1999_09 |
| ORD ID | ord-9f269605ad5e4ef8828b7ab218008c5e |
| 출처 메모 | uspto-grants-1999_09 |