Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
6-Bromohexanamide → Methyl 4-[7-(1-adamantyl)-6-carbonylpentyloxy-2-naphthyl]benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 6-Bromohexanamide | HCID 321974 | — |
| 반응물 | Methyl 4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate | HCID 22000367 | — |
| 생성물 | Methyl 4-[7-(1-adamantyl)-6-carbonylpentyloxy-2-naphthyl]benzoate | HCID 21850744 | 66% |
반응 단계
Following the procedure of Example 12(a), but reacting 640 mg (1.55 mmol) of methyl 4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate with 450 mg (2.32 mmol) of 6-bromohexanamide, 520 mg (65%) of the expected compound were obtained, which compound had a melting point of 209°-10° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05952382 |
| 출처 데이터셋 | uspto-grants-1999_09 |
| ORD ID | ord-55058d0f2c0a4a00b492fdcfcf9a0cb5 |
| 출처 메모 | uspto-grants-1999_09 |