참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Azobisisobutyronitrile | HCID 6547 | — |
| 반응물 | Acetyl bromide | HCID 10482 | — |
| 반응물 | Chrysanthemic acid, cis-(-)- | HCID 20755 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Chrysanthemic Acid | HCID 2743 | 92% |
반응 단계
5.0 g of cis-chrysanthemic acid and 0.2 g of azobisisobutyronitrile were dissolved in 50 ml of toluene and thereto was added dropwise a solution of acetyl bromide (55 mg) in toluene with stirring at 80° C. over a period of 20 minutes. Then, the same treatment as in Example 1 was effected to obtain 4.6 g of chrysanthemic acid. The IR spectrum thereof was identical with that of chrysanthemic acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04820864 |
|---|
| 출처 데이터셋 | uspto-grants-1989_04 |
|---|
| ORD ID | ord-51ce7b83a98b48aa8da236f613663938 |
|---|
| 출처 메모 | uspto-grants-1989_04 |
|---|
