참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | Epibromohydrin | HCID 18430 | — |
| 반응물 | 3,6-Dibromocarbazole | HCID 274874 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 3,6-dibromo-9-((oxiran-2-yl)methyl)-9H-carbazole | HCID 2775473 | 66.3% |
반응 단계
Following a literature procedure (Asso, V.; Ghilardi, E.; Bertini, S.; Digiacomo, M.; Granchi, C.; Minutolo, F.; Rapposelli, S.; Bortolato, A.; Moro, S. Macchia, M. ChemMedChem, 2008, 3, 1530-1534) powdered KOH (0.103 g, 1.85 mmol) was added to a solution of 3,6-dibromocarbazole (0.500 g, 1.54 mmol) in DMF (1.5 mL) at ambient temperature and stirred for 30 min until dissolved. Epibromohydrin (0.32 mL, 3.8 mmol) was added via syringe and the reaction was stirred at room temperature overnight. Upon completion, the solution was partitioned between EtOAc and H2O. The aqueous layer was washed 3× with EtOAc, and the combined organics were washed with saturated aqueous NaCl, dried over Na2SO4, filtered, and concentrated in vacuo. The crude residue was recrystallized from EtOAc/Hexane to afford the desired product (389 mg, 66%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US09446022B2 |
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| 출처 데이터셋 | uspto-grants-2016_09 |
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| ORD ID | ord-53976dd4c749409184512d631df592b6 |
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| 출처 메모 | uspto-grants-2016_09 |
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