참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Lithium Hydroxide | HCID 3939 | — |
| 반응물 | Methyl Stearate | HCID 8201 | — |
| 반응물 | (1-2-Hydroxyethyl)-2,2,6,6-tetramethyl-4-hydroxymethyl-piperidine | HCID 53937473 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 1-(2-Stearoyloxyethyl)-2,2,6,6-tetramethyl-4-methyl piperidine stearate | HCID 21292218 | — |
반응 단계
9.8 g of 1-(2-hydroxyethyl)-2,2,6,6-tetramethyl-4-hydroxymethyl piperidine as obtained in Example 2 (0.045 mole) were admixed to 28.7 g of methyl stearate (0.09 mole) in the presence of 0.5 g of LiOH. The mixture was heated to 140° C. in a nitrogen atmosphere and was maintained under stirring until complete evolvement of the reaction methyl alcohol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04772708 |
|---|
| 출처 데이터셋 | uspto-grants-1988_09 |
|---|
| ORD ID | ord-25f8bacf134a4b57be107a0a1eefb2ff |
|---|
| 출처 메모 | uspto-grants-1988_09 |
|---|
