Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cyclohexane → Spiro[cyclohexane-1,9'-fluorene]
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cyclohexane | HCID 8078 | — |
| 촉매 | HCID 178503044 | HCID 178503044 | — |
| 생성물 | Spiro[cyclohexane-1,9'-fluorene] | HCID 12861606 | — |
반응 단계
110 g of spiro[cyclohexane-1,9'-fluorene] obtained in the above (1), 100 ml of cyclohexane solvent and 20 g of 5% ruthenium-carbon catalyst (manufactured by Japan Engelhard Co.) were charged in an autoclave of 1 liter and hydrogenation was effected with a hydrogen pressure of 80 kg/cm2G at 170° C. for 5 hours.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04774013 |
| 출처 데이터셋 | uspto-grants-1988_09 |
| ORD ID | ord-898e96dc55a24a45876203d87c37ab65 |
| 출처 메모 | uspto-grants-1988_09 |