Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Bromo-2-chloro-6-methylpyridine → HCID 90202624, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Bromo-2-chloro-6-methylpyridine | HCID 2734418 | — |
| 반응물 | 3-Oxetanone | HCID 15024254 | — |
| 생성물 | HCID 90202624 | HCID 90202624 | 71% |
반응 단계
In analogy to the procedure described in Example 130 a), 3-bromo-2-chloro-6-methylpyridine (CAN 185017-72-5, 5 g, 24.2 mmol) was reacted with oxetan-3-one (CAN 6704-31-0, 1.75 g, 1.42 mL, 24.2 mmol) to give the title compound (3.42 g, 71%) as off-white solid, MS (ESI): m/e=200.5 [MH+].
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09303012B2 |
| 출처 데이터셋 | uspto-grants-2016_04 |
| ORD ID | ord-6e94af4091a6499abe54c42ce8a01fc4 |
| 출처 메모 | uspto-grants-2016_04 |