참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | p-Toluenesulfonic acid | HCID 6101 | — |
| 반응물 | Galactaric acid | HCID 3037582 | — |
| 촉매 | HCID 178477782 | HCID 178477782 | — |
| 용매 | Heptanol | HCID 8129 | — |
| 생성물 | Diheptyl galactarate | HCID 131737197 | — |
반응 단계
In one specific embodiment of the present disclosure, 20 ml of 1-heptanol, 1 mmol of galactaric acid, 0.05 mmol of methyltrioxorhenium catalyst, and 0.05 mmol of para-toluenesulfonic acid were poured into a 50 cc reactor. The temperature in the reactor was then raised to 150° C. and the reaction was performed for 12 hours, maintaining the reactor temperature at 150° C. to obtain diheptyl galactarate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US09447012B2 |
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| 출처 데이터셋 | uspto-grants-2016_09 |
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| ORD ID | ord-f5e7bc175fbd42759b8032b4cebdc309 |
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| 출처 메모 | uspto-grants-2016_09 |
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