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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 62569생성일: 2026년 10월 24일

p-Toluenesulfonic acid → Diheptyl galactarate

https://huagongshe.com/ko/reaction/62569

반응식

참여 물질

역할이름HCID투입량
반응물p-Toluenesulfonic acidHCID 6101—
반응물Galactaric acidHCID 3037582—
촉매HCID 178477782HCID 178477782—
용매HeptanolHCID 8129—
생성물Diheptyl galactarateHCID 131737197—

반응 조건

온도150 °C

반응 단계

In one specific embodiment of the present disclosure, 20 ml of 1-heptanol, 1 mmol of galactaric acid, 0.05 mmol of methyltrioxorhenium catalyst, and 0.05 mmol of para-toluenesulfonic acid were poured into a 50 cc reactor. The temperature in the reactor was then raised to 150° C. and the reaction was performed for 12 hours, maintaining the reactor temperature at 150° C. to obtain diheptyl galactarate.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US09447012B2
출처 데이터셋uspto-grants-2016_09
ORD IDord-f5e7bc175fbd42759b8032b4cebdc309
출처 메모uspto-grants-2016_09