Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cyclohexylamine → 8-Methylnonanoic acid cyclohexylamine salt
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cyclohexylamine | HCID 7965 | — |
| 반응물 | 8-Methylnonanoic acid | HCID 111470 | — |
| 용매 | Heptane | HCID 8900 | — |
| 생성물 | 8-Methylnonanoic acid cyclohexylamine salt | HCID 68605324 | — |
반응 단계
From the 8-methylnonanoic acid crude product obtained in Example 1, 8.00 g was dissolved in heptane (30 ml). Cyclohexylamine (6.91 ml, 60.4 mmol) was slowly added dropwise at 0° C. (ice bath), and the mixture was stirred at room temperature for 20 minutes. The reaction mixture was filtered to give 8-methylnonanoic acid cyclohexylamine salt (15.7 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07700331B2 |
| 출처 데이터셋 | uspto-grants-2010_04 |
| ORD ID | ord-f0e91b54879e4f9caeab73e5e708080f |
| 출처 메모 | uspto-grants-2010_04 |